Titration to calculate the water of crystallisation

You have read the exam question carefully and decided that the following are the key bits of information:

  • 3.69 g of Ba(OH)2.xH2O is made into a 250 cm3 solution
  • A 25 cm3 sample of the solution is titrated with 23.4 cm3 of 0.1 mol/dm3 HCl.
  • Calculate the relative formula mass of Ba(OH)2.xH2O, and hence x.
Step 1

We know that moles = concentration x volume:

n HCl = 0.1 x (23.4 / 1000) =  2.34 x 10-3 mol.

Step 2

The balanced symbol equation isn’t given so we need to work it out. This is an acid-base reaction neutralisation:

2 HCl + Ba(OH)2 –> BaCl2 + 2 H2O

Step 3

The molar ratio is 2:1 so this means the moles of Ba(OH)2 that reacted in the sample was:

n Ba(OH)2 = 1/2 x 2.34 x 10-3 mol = 1.17 x 10-3 mol

Step 4

The total is 10x bigger than the sample (i.e., 250 / 25):

n Ba(OH)2 = 10 x 1.17 x 10-3 mol = 1.17 x 10-2 mol in total

Step 5

This means that the Mr of Ba(OH)2.xH2O is:

Mr Ba(OH)2.xH2O = 3.69 / 1.17 x 10-2 = 315

Step 6

We can now subtract the Mr of just Ba(OH)2 (Mr = 171)

Mr xH2O = 315 – 171 = 144

Step 7

We can now divide by 18 (the Mr of H2O) to find x

x = 144 / 18 = 8