Titration to identify the element M

You have read the exam question carefully and decided that the following are the key bits of information:

  • 3.69 g of soluble M2CO3 is made into a 250 cm3 solution
  • A 25 cm3 sample of the solution is titrated with 26.7 cm3 of 0.2 mol dm-3 HNO3.
  • Calculate the relative atomic mass of M, and hence, identify the element M.
Step 1

We know that moles = concentration x volume:

n HNO3 = 0.2 x (26.7 / 1000) =  5.34 x 10-3 mol.

 

Step 2

The balanced symbol equation isn’t given so we need to work it out. The only thing that we know about M is that it has a 1+ charge. You might guess that it is probably a Group 1 metal, especially as we’re told it’s a soluble carbonate. We can therefore write down the balanced symbol equation:

2 HNO3 + M2CO3 –> 2 MNO3 + H2O + CO

 

Step 3

The balanced symbol equation tells us that HNO3 and M2CO3 react in a 2:1 ratio so the M2CO3 moles in the sample is:

n M2CO3 = 0.5 x 5.34 x 10-3 mol = 2.67 x 10-3 mol

 

Step 4

The total is 10x bigger than the sample (i.e., 250 / 25) so we can work out the initial M2CO3 moles:

n M2CO3 = 10 x 2.67 x 10-3 = 2.67 x 10-2 mol

 

Step 5

We have the mass of M2CO3 (3.69 g) and can assume that it is pure. This means that the Mr of M2CO3 is:

Mr M2CO3 = 3.69 / 2.67 x 10-2 = 138.2

 

Step 6

The Ar of M can then be found by subtracting the mass of CO3 (60) from the Mr to find the mass of just M2 (138.2 – 60 = 78.2).

The Ar of M is therefore 78.1 / 2 = 39.1

The closest match on the periodic table is potassium (K).

You might want to think about why this approach wouldn’t work for Group 2 carbonates?… The answer is that they are all insoluble. In this case, we would need to do a back titration.